Correlation of 13C and 1H chemical shifts in bovine high-density lipoprotein from two-dimensional NMR

Scott Coffin, Mona Limm, David Cowburn

Research output: Contribution to journalArticle

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Abstract

Two-dimensional heteronuclear 13C1H chemical-shift correlation spectra were obtained for bovine high-density lipoprotein (HDL). The 13C and 1H shifts of the lipid components are assigned. No evidence for dynamic equilibration of lipid classes between different structure environments was found at this limited resolution. Heteronuclear correlation spectroscopy can be effectively applied to macromolecular complexes as large as HDLs.

Original languageEnglish (US)
Pages (from-to)268-274
Number of pages7
JournalJournal of Magnetic Resonance (1969)
Volume59
Issue number2
DOIs
Publication statusPublished - Sep 1984
Externally publishedYes

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