Correlation of 13C and 1H chemical shifts in bovine high-density lipoprotein from two-dimensional NMR

Scott Coffin; Mona Limm; David Cowburn

doi:10.1016/0022-2364(84)90171-9

Correlation of ¹³C and ¹H chemical shifts in bovine high-density lipoprotein from two-dimensional NMR

Scott Coffin, Mona Limm, David Cowburn

Research output: Contribution to journal › Article › peer-review

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Abstract

Two-dimensional heteronuclear ¹³C¹H chemical-shift correlation spectra were obtained for bovine high-density lipoprotein (HDL). The ¹³C and ¹H shifts of the lipid components are assigned. No evidence for dynamic equilibration of lipid classes between different structure environments was found at this limited resolution. Heteronuclear correlation spectroscopy can be effectively applied to macromolecular complexes as large as HDLs.

Original language	English (US)
Pages (from-to)	268-274
Number of pages	7
Journal	Journal of Magnetic Resonance (1969)
Volume	59
Issue number	2
DOIs	https://doi.org/10.1016/0022-2364(84)90171-9
State	Published - Sep 1984
Externally published	Yes

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10.1016/0022-2364(84)90171-9

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@article{c392c73d81a44339ab66e6c0dc69acb7,

title = "Correlation of 13C and 1H chemical shifts in bovine high-density lipoprotein from two-dimensional NMR",

abstract = "Two-dimensional heteronuclear 13C1H chemical-shift correlation spectra were obtained for bovine high-density lipoprotein (HDL). The 13C and 1H shifts of the lipid components are assigned. No evidence for dynamic equilibration of lipid classes between different structure environments was found at this limited resolution. Heteronuclear correlation spectroscopy can be effectively applied to macromolecular complexes as large as HDLs.",

author = "Scott Coffin and Mona Limm and David Cowburn",

note = "Funding Information: This research was supported by American Heart Association Grant in Aid 82 1099 and NIH AM-20357, RR-07065. SC. is a NSF Graduate Fellow. We are grateful to Professor Donald McNamara, and to Professor John B. Swaney, Albert Einstein College of Medicine, for advice on HDL preparations.",

year = "1984",

month = sep,

doi = "10.1016/0022-2364(84)90171-9",

language = "English (US)",

volume = "59",

pages = "268--274",

journal = "Journal of Magnetic Resonance (1969)",

issn = "0022-2364",

publisher = "Academic Press Inc.",

number = "2",

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T1 - Correlation of 13C and 1H chemical shifts in bovine high-density lipoprotein from two-dimensional NMR

AU - Coffin, Scott

AU - Limm, Mona

AU - Cowburn, David

N1 - Funding Information: This research was supported by American Heart Association Grant in Aid 82 1099 and NIH AM-20357, RR-07065. SC. is a NSF Graduate Fellow. We are grateful to Professor Donald McNamara, and to Professor John B. Swaney, Albert Einstein College of Medicine, for advice on HDL preparations.

PY - 1984/9

Y1 - 1984/9

N2 - Two-dimensional heteronuclear 13C1H chemical-shift correlation spectra were obtained for bovine high-density lipoprotein (HDL). The 13C and 1H shifts of the lipid components are assigned. No evidence for dynamic equilibration of lipid classes between different structure environments was found at this limited resolution. Heteronuclear correlation spectroscopy can be effectively applied to macromolecular complexes as large as HDLs.

AB - Two-dimensional heteronuclear 13C1H chemical-shift correlation spectra were obtained for bovine high-density lipoprotein (HDL). The 13C and 1H shifts of the lipid components are assigned. No evidence for dynamic equilibration of lipid classes between different structure environments was found at this limited resolution. Heteronuclear correlation spectroscopy can be effectively applied to macromolecular complexes as large as HDLs.

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U2 - 10.1016/0022-2364(84)90171-9

DO - 10.1016/0022-2364(84)90171-9

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JO - Journal of Magnetic Resonance (1969)

JF - Journal of Magnetic Resonance (1969)

IS - 2

ER -

Correlation of ¹³C and ¹H chemical shifts in bovine high-density lipoprotein from two-dimensional NMR

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